Prelaboratory Assignment and Lab Notebooks
Prior to coming to lab, it is your responsibility to read
the entire laboratory experiment and procedure so that you know what you will
be doing and how you will be doing it. To aid you in this, you will need
to prepare your laboratory notebook before each experiment. The
preparation of your lab notebook will constitute your prelab
assignment.
Getting your lab notebook ready should not be mere
busy-work that you complete in the few minutes before lab. The more
prepared you are for the lab ahead of time, the more smoothly the lab will run
and the more you will get out of it. In addition, it will make writing
the laboratory report much easier.
The prelaboratory
assignment will be checked at the beginning of each lab period. If yours
is not complete, you will not be allowed to begin the experiment until it
is. The following information should be in your notebook for each
experiment (as appropriate).
- Number each page. Allow space at the front of the
notebook for a table of contents. Use a hardbound (not spiral-bound),
lined notebook, and keep all notes in ink. You may continue using
this notebook if you take Chem 1062.
- Date each entry, starting on a fresh right-hand
page. Often it is common to use only the right-hand page when
entering information.
- Give a short title to the experiment, and enter it in
the table of contents.
- Technical details should be recorded (or space for
them provided). These details include information like lab partner’s
name, instructor name, and the file name given to the data.
- With the technical details taken care of, it is time
to write down some of the what’s and why’s
associated with the experiment. To begin with, state the purpose or
problem of the experiment as you understand it. What are we trying to
accomplish? What are we going to
learn?
- When appropriate, include a working hypothesis
regarding the outcome of the experiment. This is also a point where
you may jot down questions that you have about the lab. These
questions may be about how something is done, why something is done, or
what type of information one could expect to get. They could also be
about how things will look or what will be observed.
- Briefly summarize
the course of action or procedure that will be used to satisfy number
5 above or reference the URL for
the lab if the procedure is included in the lab. In your procedure, note any hazards and
safety precautions. If severe, make them bold or circled. State how all waste will be
disposed of. Usually we will have appropriate waste containers but often
the procedure will require special waste disposal procedures
(neutralizations, etc).
- Prepare a table of quantities (mmols,
concentration, g, mL, as needed) of each
chemical required in the lab experiment. Leave room in this table to write
the amount you actually use.
During the Lab
1. Don’t forget to record all your observations
as they happen. If you make a mistake, DO NOT erase
it or scribble it out. Instead, place a single line through it, initial
beside it, and continue on.
2. Record all data (masses, appearances of
product, and anything that happens in the reaction itself) in your lab book. Do
not write data on scratch paper and then transfer into your book – use the blank
left-hand pages for scratch notes and calculations. If data is recorded
on the computer, print out the tables or
graphs and tape them into your lab notebook on either the left or right page.
This part may need to be done after lab for some of the experiments.
3. When you are finished gathering and analyzing
data, you need to have your lab notebook witnessed. This can be
done by your lab partner, lab instructor, or the laboratory manager. As a
witness, the person will sign and date your notebook after the last thing recorded for
that lab.